Synthesis of New Derivative of Adipoyl Thiadiazole
Abstract
This research includes the preparation of new derivatives of adipoyl thiadiazoles, through the reaction of each of hydrazine hydrate , phenyl hydrazine , 2,4-dinitrophenyl hydrazine, semicarbazide and thiosemicarbazid with adipoly chloride in the presence of ethanol (95%). Furthermore, thiadiazoles were made through cyclization of hydrazine , semicarbazide and thiosemicarbazid in alkaline media, such as potassium hydroxide solution in presence of carbon disulfide. The prepared compounds were identified by the physical and spectroscopic methods
Keywords
Thiadiazole, hydrizides, semicarbazide, thiosemicarbazide, adipoly chloride, Carbon disulfide .Metrics