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SYNTHESIS AND CHARACTERIZATION OF SOME METAL IONS WITH {[5-(4-CHLOROPHENYL)-1,3,4-OXADIAZOL-2-YL]THIO} ACETIC ACID

Authors: Emad Yousif --- Eva Rentschler
Journal: Al-Nahrain Journal of Science مجلة النهرين للعلوم ISSN: (print)26635453,(online)26635461 Year: 2010 Volume: 13 Issue: 2 Pages: 86-92
Publisher: Al-Nahrain University جامعة النهرين

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Abstract

New metal complexes of the ligand {[5-(4-chlorophenyl)-1,3,4-oxadiazol-2-yl]thio}acetic acidwith the metal ions Ni(II), Cu(II), Zn(II), Cd(II) and Sn(II) were prepared in alcoholic medium. Theprepared complexes were characterized by FTIR Spectroscopy, electronic spectroscopy 1HNMR,13CNMR, magnetic susceptibility and conductivity measurements. From the spectral measurements,monomer structures for the complexes were proposed. Square planar geometry was proposed forthe copper complex. The other complexes were proposed to be tetrahedral

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