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Preparation and Characterization of TiO2 Nanostructure by TiCl4 Hydrolysis with Additive NaOH

Author: Rashed Taleb Rasheed
Journal: Al-Mustansiriyah Journal of Science مجلة علوم المستنصرية ISSN: 1814635X Year: 2017 Volume: 28 Issue: 2 Pages: 100-107
Publisher: Al-Mustansyriah University الجامعة المستنصرية

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Abstract

Titanium dioxide (TiO2) nanostructures were synthesized via the hydrolysis of TiCl4 in alcohol /water solution/with sodium hydroxide solution in the ice-bath (0-5 ◦C). The particles were characterizedby using X-ray diffraction technique (XRD), spectroscopy of Ultra Violet-Visible (UV/ Visible) and infrared (FT-IR), atomic force microscope (AFM) and scanning electron microscope(SEM) analysis were used in order to gain information about the material, morphology,size and the shape of the particles.

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